潘世光,硕士生导师,博士毕业于日本早稻田大学(Waseda University),师从Takanori Shibata教授,长期致力于高性能非均相催化剂可控构筑与应用、纳米多孔金属/金属基催化材料的开发。曾担任国际化学评论期刊Synfacts杂志撰写人,现任职于天津工业大学。曾获日本学术振兴会特别研究员 (JSPS)、中国国家优秀自费留学生等荣誉。主持日本文部省和天津市项目各1项,申请发明专利多项。以第一作者在Journal of The American Chemical Society、ACS Catalysis、Organic Letters等国内外高水平期刊上发表研究论文二十余篇,论文累计他引1300余次,其中高被引论文1篇。
目錄:
Chapter 1General Knowledge of Organic Chemistry Experiments(1)
1.1Laboratory rules(1)
1.2Prevention and treatment of experimental accidents(2)
1.3Experiment record and experiment report(7)
1.4Check items if the experiment does not give results(9)
1.5Glassware commonly used in organic chemistry laboratories(10)
1.6Methods of cleaning, drying, and maintaining the instruments(15)
1.7Application of lowtemperature refrigeration(19)
1.8Commonly heating appliances and equipment(19)
Chapter 2Basic Operation and Experimental Technology of Organic Chemistry Experiment(23)
2.1Determination of physical constants of organic compounds(23)
2.2Simple glazier operation(28)
2.3Cooling and heating(31)
2.4Separation and purification of organic compounds(34)
2.5Drying and the use of desiccant(60)
Chapter 3Experiments(64)
3.1Distillation of saturated aqueous solution of nbutanol(64)
3.2Synthesis of 1bromobutane(68)
3.3Synthesis of ethyl acetate(72)
3.4Synthesis of nbutyl acetate(75)
3.5Synthesis of ethyl benzoate(77)
3.6Synthesis of nbutyl ether(81)
3.7Synthesis of acetanilide(83)
3.8Recrystallization of acetanilide(85)
3.9Synthesis of pbromoacetanilide(88)
3.10Synthesis of benzyl alcohol and benzoic acid(90)
3.11Synthesis of αfuryl methanol and αfuroic acid(93)
3.12Synthesis of benzyl alcohol(95)
3.13Synthesis of benzoic acid(97)
3.14Synthesis of cyclohexene(99)
3.15Synthesis of cyclohexanone(101)
3.16Synthesis of cinnamic acid(104)
3.17Synthesis of acetylsalicylic acid(106)
3.18Synthesis of 2methyl2butanol(108)
3.19Synthesis of tertbutylhydroquinone(112)
3.20Synthesis of nitrobenzene(114)
3.21Synthesis of adipic acid(117)
3.22Synthesis of dimethyl adipate(119)
3.23Comprehensive experiment: green synthesis of 2,2′furil(121)
Chapter 4Appendix(127)
4.1List of the element with their symbols and atomic masses(127)
4.2Structures and names for common solvents used in organic chemistry(131)
4.3Properties for common solvents used in organic chemistry(132)
4.4Cooling baths(132)
4.5Common azeotropes(133)
4.6Pressuretemperature nomograph(134)
4.7Periodic table(134)