上篇 中 文 部 分
章基础化学实验须知(3)
节实验守则(3)
第二节基本知识(9)
第三节基本技能(27)
第四节实验误差、数据处理和实验报告(43)
第二章基础化学实验部分(48)
实验一玻璃仪器认领、清洗、干燥及实验数据的处理方法(48)
实验二气体常数R的测定(49)
实验三凝固点降低法测定溶质的相对分子质量(51)
实验四酸、碱标准溶液的配制及其浓度的比较(53)
实验五乙酸解离度与解离常数的测定(56)
实验六化学反应速率与活化能的测定(58)
实验七有机酸试剂纯度的测定(62)
实验八APC药片中阿司匹林含量的测定(64)
实验九混合碱的分析(66)
实验十消毒液中H2O2含量的测定(69)
实验十一注射液中葡萄糖含量的测定(71)
实验十二自来水总硬度的测定(73)
实验十三同离子效应与沉淀平衡(76)
实验十四缓冲溶液的配制与性质(79)
实验十五氧化还原反应和电极电位(82)
实验十六配合物的生成和性质(85)
实验十七过渡金属化合物的性质与应用(88)
实验十八蛋白质的分光光度法测定(93)
实验十九磺基水杨酸合铁(Ⅲ)配合物的组成和稳定常数的测定(95)
实验二十分光光度法测定\\[Ti(H2O)6\\]3 的晶体场分裂能(97)
实验二十一生理盐水中氯离子含量的测定(99)
实验二十二食品中亚硝酸盐含量的测定(100)
实验二十三双波长分光光度法测定水样中硝酸盐的含量(102)
实验二十四火焰原子吸收光谱法测定人头发中的锌(104)
实验二十五荧光分光光度法测定牛奶中的核黄素(105)
实验二十六pH玻璃电极性能检查及饮料pH的测定(107)
实验二十七电导法测定水质纯度(109)
实验二十八氟离子选择电极法测定水样中氟离子的浓度(110)
实验二十九气相色谱法测定废水中的苯系物(112)
实验三十高效液相色谱法测定食品中的色素(113)
实验三十一粗食盐的提纯(115)
实验三十二硫酸亚铁铵的制备(含微型实验)(117)
实验三十三溶胶的制备和性质(120)
实验三十四水热法制备纳米SnO2微粉(122)
实验三十五茶叶中微量元素的鉴定与定量测定(125)
综合性实验(一)葡萄糖酸锌的制备及锌含量的测定(128)
综合性实验(二)三草酸合铁(Ⅲ)酸钾的合成及组成测定(129)
综合性实验(三)蛋壳中钙、镁含量的测定(131)
设计性实验(一)钴(Ⅲ)配合物的制备及其组成的确定(134)
设计性实验(二)水样中铁含量的测定(135)
设计性实验(三)果蔬中维生素C含量的测定(136)
设计性实验(四)植物中某些元素的鉴定(137)
趣味性实验(138)
下篇 英 文 部 分
Part OneIntroduction of BasicChemistry Experiments(143)
Chapter 1Basic Rules and Safety Requirements (143)
Chapter 2Common Laboratory Techniques andPractices(151)
Chapter 3Weighing with Balances(174)
Chapter 4Basic Operation of Volumetric Glassware(179)
Chapter 5pH Meter(187)
Chapter 6Instructions for 723N Spectrophotometer(191)
Chapter 7Evaluation of Experimental Data(193)
Part TwoExperiments in Basic Chemistry(203)
Experiment 1Measurements,Common LaboratoryTechniques and
Practices(203)
Experiment 2Determination of the Gas Constant(205)
Experiment 3Determination of the Relative Molecular Weight of Solute
by Freezing Point Depression(207)
Experiment 4Preparation and Comparison of Acidand Base Standard
Solutions(209)
Experiment 5Determination of the Ionization Degree and Ionization
Constant of Acetic Acid(212)
Experiment 6Determination of a Rate Law andActivation Energy(215)
Experiment 7Determination of the Purity of an Unknown Acid(218)
Experiment 8Determination of Aspirin in Aspirin Tablets(221)
Experiment 9Determination of the Composition of a CarbonateBicarbonate
Mixture(223)
Experiment 10Determination of Hydrogen Peroxidein Nosocomial
Disinfector(226)
Experiment 11Iodimetric Determination of Glucose in Nosocomial
Injection(229)
Experiment 12Determination of Water Hardness Using Complexometric
Titration(232)
Experiment 13The Common Ion Effect and Precipitation Equilibrium(235)
Experiment 14Preparation and Properties of Buffer Solutions(239)
Experiment 15OxidationReduction Reaction andElectrode Potential(242)
Experiment 16Preparation and Properties of Coordination
Compounds(246)
Experiment 17Transition Metals(251)
Experiment 18Spectrophotometric Determinationof Protein in Peanut(259)
Experiment 19Determination of the Composition and the Stability Constant
for anIron(Ⅲ)Sulfosalicylate Complex(261)
Experiment 20Spectrophotometric Determination of Crystal Field Splitting
Energy of \\[Ti(H2O)6\\]3 (264)
Experiment 21Measurement of Chloride Ion Content in Saline(266)
Experiment 22Measurement of Nitrite Concentration in Food(268)
Experiment 23Determination of Nitrate Content in Water Samples by
Dualwavelength Spectrophotometry(270)
Experiment 31Purification of Sodium Chloride(272)
Experiment 25Determination of Riboflavin in Milk by Fluorimetry(274)
Experiment 26The Inspection of the Perfermance of the Glass
Electrode and the Determination of the pH
Value of a Beverage(276)
Experiment 27Determination of Water Purity by Conductometry(278)
Experiment 28Determination of Fluorine Ion in Water by Fluoride
Ionselective Electrode(280)
Experiment 29Determination of Benzene Series in WasteWater by Gas
Chromatography(282)
Experiment 30Determination of Pigments in Food by HPLC(284)
Experiment 31Purification of Sodium Chloride(287)
Experiment 32Synthesis of Ferrous Ammonium Sulfate(289)
Experiment 33Preparation and Properties of the Colloid(292)
Experiment 34Preparation of Tin Dioxide Nanopowder by Hydrothermal
Method(295)
Experiment 35Determination of Trace Elements in Tea(299)
Experiment 36Preparation of Zinc Gluconate and Complexometric
Titrationof Zinc with EDTA(303)
Experiment 37Preparation and Analysis of PotassiumTris(oxalato)ferrate
(Ⅲ)Trihydrate,K3 \\[Fe(C2O4)3\\]·3H2O(305)
Experiment 38Titration of an Eggshell(308)
Experiment 39Synthesis of Cobalt(Ⅲ)Coordination Compounds(311)
Experiment 40Determination of Fe in Water Sample(314)
Experiment 41Determination of Vitamin C in Juices(317)
Experiment 42Determination of Some Elements in Plant(320)
附录A元素相对原子质量表(323)
附录B常用指示剂(324)
附录C常用酸碱的相对密度和浓度(326)
附录D常用缓冲溶液的配制(326)
附录E常用一级标准物质的干燥条件和应用(327)
附录F常用试剂的配制(328)
附录G化学手册简介(329)
参考文献(331)