第一章 中药制剂分析实验的基本知识
Chapter 1 Elementary Knowledge of Experiment for Analysis of Traditional Chinese Medicine Preparation
第一节 中药制剂分析实验基本要求及注意事项
Section 1 Basic Requirements and Announcements of Experiment for Analysis of Traditional Chinese Medicine Preparation
第二节 供试品溶液的制备
Section 2 Preparation of Test Solution
第三节 分析方法验证的基本内容
Section 3 The Basic Content of Analysis Method
第四节 实验记录与报告
Section 4 Experimental Record and Report
第二章 中药制剂分析实验
Chapter 2 Experiment for Analysis of Traditional Chinese Medicine Preparation
单项实验 Individual Experiment
实验一 五苓散与万氏牛黄清心丸的显微鉴别
Experiment 1 Microscopical Identification of Wuling Powder and Wanshi Niuhuang Qingxin Pills
实验二 安胃片与冰硼散的理化鉴别
Experiment 2 Physical—-Chemical Identification of Anwei Tablets and Bingpeng Powder
实验三 桂枝茯苓丸与葛根芩连片的薄层色谱鉴别
Experiment 3 Identification of Guizhi Fuling Pills and Gegen Qinlian Tablets by TLC
实验四 附子理中丸中乌头碱及砷盐的限量检查
Experiment 4 Limit Test of Aconitine and Arsenate in Fuzi Lizhong Pills
实验五 甲苯法测定通宣理肺丸中的水分
Experiment 5 Determination of Water in Tongxuan Lifei Pills
实验六 气相色谱法测定藿香正气水中乙醇的含量
Experiment 6 Determination of Ethanol in Huoxiang Zhengqi Tincture by GC
实验七 黄连上清丸中重金属的检查
Experment 7 Test of Heavy Metals in Huanglian Shangqing Pills
实验八 酸性染料比色法测定华山参片总生物碱的含量
Experiment 8 Determination of the Total Alkaloids in Tabellae Physochlainae by Acid-dye Colorimetry
实验九 气相色谱法测定西瓜霜润喉片中冰片的含量
Experiment 9 Determination of Borneolum Syntheticum in Xiguashuang Runhou Tablets by GC
实验十 HPLC法测定逍遥丸中芍药苷的含量
Experiment 10 Determination of Paeoniflorin in Xiaoyao Pills by HPLC
实验十一 HPLC法测定银杏叶片中总黄酮醇苷的含量
Experiment 11 Determination of Total Amount of Flavonol Glycosides in Yinxingye Tablets by HPLC
实验十二 注射用益气复脉冻干的HPLC指纹图谱
Experiment 12 HPLC fingerprint chromatography of Yiqifumai Injection
实验十三 “一测多评”法测定三黄片中4种黄芩黄酮类成分
Experiment 13 Determination of four kinds of Scutellaria flavonoids in Sanhuang Tablets by QAMS
综合性实验Comprehensive Experimemt
实验十四 二妙丸的鉴别与挥发油的测定
Experiment 14 Identification of Ermiao Pills and Determination of Volatile Oil
实验十五 大山楂丸的鉴别与总黄酮的含量测定
Experiment 15 Identification of Dashanzha Pills and Determination of Total Flavonoids
实验十六 注射用双黄连冻干的质量分析
Experiment 16 Quality Analysis of Shuanghuanglian for Injection
实验十七 六味地黄丸的质量分析
Experiment 17 Quality Analysis of Liuwei Dihuang Pills
设计性实验Design Experiment
实验十八 设计复方丹参片的质量分析方法
Experiment 18 Design the Analysis Experiment for Compound Salvia Tablets
实验十九 设计消渴丸的质量分析方法-
Experiment 19 Design of Analysis Experiment for Xiaokewan Pills
实验二十 设计牛黄解毒片的质量分析方法
Experiment 20 Design of Analysis Experiment for Niuhuang Jiedu Tablets
附录 常用薄层色谱显色剂的配制和使用
Appendix The preparation and usage of commonly used TLC colorant